Page 457 - Applied Pharmacognosy
P. 457

b- Gas chromatographic method

• The water in a weighed powdered sample is extracted
  with dry or anhydrous methanol.

• An aliquot is submitted to GLC using quantitation by the
  internal standard method

• (n-propanol as internal standard) the apparatus is
  equipped with TCD. (Thermal conductivity detector)

•                                          R = relative response
                       u = sample solution
s = standard solution
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