Page 60 - Practical-workbook-organic-3 isa

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1. Opening the FID of H-NMR.
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2. Identify the solvent type

3. Pick peaks (to identify the chemical shifts of all peaks of the chart).

4. Integration steps (to identify the chemical shifts of all peaks of the chart).
5. Plot layout (to save the chart as pdf of different expansions).

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Step one: Opening the FID of H-NMR from the left hand side bar (LHS)
(C:/Bruker/TopSpin3.6.2/examdata)

a. Select the required experiment name.

b. Double left click on the appeared experiment
a.
title (behind no. 10) b..
c..
c. Double left click on the appeared experiment

title (behind no. 1)

Step two: Identify the solvent type:

• Type (solvent) in the command bar and press
enter then press Ok.

• DMSO peak at 2.5 & 3.3 ppm & CDCl3 peak

at 1.6 & 7.2 ppm.

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