Page 22 - A Burning Question Fire Debris
P. 22

Lab

             Procedure








               LAB 1



               ANALYSIS OF IGNITABLE LIQUIDS PRESENT IN KNOWN
               FIRE DEBRIS SAMPLES



               1.  Prior to analyzing evidence collected from the     4. Puncture the label on the lid of the container
                 crime scene, you will practice the techniques      with the end of the colorimetric tube.
                 required to identify the presence of ignitable
                 liquids in non-evidentiary known samples          5. Carefully break both ends off of the tube
                 of fire debris. When breaking the ends off of      being used by inserting the tube end
                 colorimetric tubes, glass edges may be sharp       through the colorimetric tube opener to just
                 so great care must be taken when handling          past the ball. With the tube pointed away
                 fragments. Do not handle glass fragments           from your body, grasp the side of the tube
                 without wearing proper personal protective         opener and twist downward to break the end
                 equipment, including gloves and goggles.           off of the tube.


               2.  Determine which groups will perform which       6. Carefully insert the colorimetric tube
                 analysis - three groups will analyze the samples   through the lid. Ensure that the arrow on
                 for the presence of gasoline and three groups      the tube (indicating direction of airflow)
                 will analyze the samples for the presence of       is pointed toward the outside of
                 diesel fuel.                                       the container.

               3.  Select the sample container and colorimetric     7.  Roll a small piece of colorimetric tube sealant
                 tube appropriate for analysis (Ex. gasoline        into a rope and use this to seal the opening
                 spiked sample and gasoline colorimetric tube)      between the tube and the lid. Ensure no
                 and ensure the lid is securely tightened onto      openings remain that would allow vapors to
                 the container.                                     escape.






              22    THE MYSTERY OF LYLE AND LOUISE
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