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plating and anodizing: CHROME REGULATIONS


                 New Chromium Electroplating,


                 Chromium Anodizing and Reverse



                 Etching Regulations Take Effect




                 BY STEWART TYMCHUK
                 sor/2009-162
                 Recently, the Chromium Electroplating, Chromium Anodiz-
                 ing and Reverse Etching Regulation was amended. The
                 goals of the regulatory amendments were to both provide
                 more flexibility and consistency for facilities to comply
                 with the Regulations and to clarify regulatory requirements
                 in light of currently available technologies.
                    In essence, the Regulations previously required surface
                 tension measurements be made with a tensiometer and
                 be performed in accordance with ASTM D 1331-89
                 (re-approved 2001), Standard Test Methods for Surface
                 and Interfacial Tension of Solutions of Surface-Active
                 Agents. New and different types of tensiometers are now
                 available which are not based on the principles of the du
                 Nouy tensiometer and therefore do not require a reference
                 to ASTM D 1331-89.

                 aPPlication
                                                                     The Kibiron AquaPi+ is one example of
                 These regulations apply to any facility that uses a solution  a high precision tensiometer which can now be used
                 containing a hexavalent chromium compound for       under the new regulations for more reliable, faster, and precise measurements.
                 chromium electroplating, chromium anodizing or reverse
                 etching in a tank where 50 kg or more of chromium trioxide
                 (CrO3) is used per calendar year.                   (4) Each facility intending to change either the method
                                                                        of controlling the release of hexavalent chromium
                 General reqUirements                                   compounds from a tank or the surface tension meas-
                 (1) Each facility, where the regulation applies, must con-  urement method for a tank must notify the Ministry.
                     trol the release of hexavalent chromium compounds
                     from each tank by one of the following methods:  Use of a Point soUrce
                    • using a point source;                          Each facility that controls the release of hexavalent
                    • limiting the surface tension of the solution   chromium compounds from a tank by using a point source
                      in the tank;                                   must use a control device in the emission collection system
                    • using a tank cover.                            and must not release more than 0.03 mg/dscm of hexavalent
                                                                     chromium from any point source.
                 (2) Each facility must submit a notice to the Minister   Each facility required to comply must perform a release
                     indicating, for each tank, the method used to control  test establishing compliance at each point source and per-
                     the release of hexavalent chromium compounds.   form a new release test at least every five years afterwards,
                                                                     providing the average of three sampling runs from that test
                 (3) If the release of hexavalent chromium compounds  did not exceed 0.03 mg/dscm of hexavalent chromium
                     from a tank is controlled by limiting the surface   from any point source.
                     tension of the solution, the notice must state whether  These tests must be repeated if the facility has replaced
                     a tensiometer or a stalagmometer is or will be used  a control device, increased the total surface area of the
                     to measure surface tension.                     solution by more than 25 percent or made changes to
                                                                     the ventilation system that affected the velocity or the
                                                                     flow rate.

                 www.cfcm.ca                                       canadian finishinG & coatinGs manUfactUrinG 25
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