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                                 3
                 (ii) Pipette 25cm  of solution L into 250cm  conical flask and add 2 drops of phenolphthalein
                        indicator to it and titrate with solution N.
                 (iii) Record your results in the table below
                 (iv) Repeat the experiment twice to obtain consistent readings and complete the table


             Table 1
                      Titration                            1             2                  3
                                              3
                      Final burette reading (cm )
                                               3
                      Initial burette reading (cm )
                                                    3
                      Volume of solution N used (cm )

                 (a) Calculate the average volume of solution N used
                 (b) Determine:-
                        (i) The concentration of sodium hydroxide in one litre of solution L
                             (Na =23, O= 16, H= 1)
                      (ii) Write the equation of the reaction taking place
                      (iii) The number of moles of anhydrous carbohydrates oxalic acid in one litre of the
                            solution N
                   (iv) The relative formula mass of anhydrous oxalic acid, solution N (C = 12,  H=1, O = 16)
                 (v) The number of moles of water of crystallization in one mole of oxalic acid


             2.         You are provided with solid K, a boiling tube and a thermometer. You are required to
                        determine the solubilities of solid K, at various temperatures.
                        Procedure:-
                                                                                                        3
                        (a) Carefully transfer all the 4.0g of solid K into a clean boiling tube and add 10cm  of
                            distilled water from a burette.
                 (b) Heat the boiling tube and its contents gently with shaking until all the solid dissolves.
                      (Do not spill the solution during heating.) Stop heating when all the solid dissolves.
                       See the diagram below:-





                                  Thermometer


                                                                          Test-tube holder



                                                                              Boiling tube


                                                            Heat
                 (c) Gently stir the solution using the thermometer and record the temperature at which
                      crystals appear.     (The crystals appear as small shining particles)
                                             3
                 (d) Using a burette add 2.5cm  of water to the solution and heat until all the solid dissolves.
                       Repeat procedure(c)

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