Page 154 - Chemistry
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             1.   (i) Dissolve solid M in 15cm of distilled water. Divide the resulting solution into six portions.
                          Record your observations
                 (ii) Add 3-4 drops of Lead nitrate to the first portion
                  (iii) Add 3-4 drops of Barium nitrate solution to the second portion
                 (iv) Add 3-4 drops of sodium hydroxide solution to the third portion
                 (v) Dip a glass rod into the fourth portion. Heat the end of glass rod dipped into the solution
                           in a non-luminous flame
                  (vi) Add 4 drops of acidified manganate (VII) to the fifth portion and warm the mixture

                        Q3.
                 1.     Solid Y-1spatulaful
                 2.     Solid Z-1spatulaful
                 3.     6 test tubes
                 4.     1 red + 1blue litmus papers
                 5.     Metallic spatula
                 6.     pH paper
          3.     (a) You are provided with solid Y

              You are required to:
             (i)    Carry out the test described below on solid Y
             (ii)   Record your observations and inferences
             (iii)   Test for any gas (es) produced

             Procedure-
                 (i)    Place a spatula of solid Y into a boiling
                                        3
                 (ii)   Add about 15cm  of distilled water and shake well
                 (iii)   Divide the resulting solution into five portions
                 (iv)   Use a universal indicator paper to test portion one of the solution
                 (v) Add a spatula of sodium carbonate to the second portion
                                                                                  rd
                 (vi) Add three drops of Potassium manganate (VII) solution to the 3  portion
                                                              th
                 (vii) Add three drops of bromine water to the 4  portion. Warm the mixture if necessary
                                3
                 (viii) Place 2cm  of ethanol in a test-tube. Add 2 drops of concentrated Sulphuric (VI) acid
                          and then a spatula end full of solid Y. Shake well and warm the mixture carefully, pour
                                                  3
                          the warm mixture into 25cm  of  cold water in a beaker and note the smell

                                                   MUMIAS DISTRICT

                 CONFIDENTIAL
                 INSTUCTIONS.
                 In addition to the apparatus and fittings found in the laboratory each candidate should have:
                            1.  One 25ml pipette
                            2.  One 3-way pipette filler
                            3.  One 0-50m/s Burrette
                            4.  Two 250m/s conical flask
                            5.  One 100ml measuring cylinder
                            6.  One 100ml glass beaker
                                                     o
                                                              o
                            7.  One thermometer (-10 C to 110 C)
                            8.  One stop watch / clock
                            9.  One label
                            10. One 10m/s measuring cylinder
                            11. White tile
                            12. 250ml beaker

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