Page 172 - Chemistry

INSTRUCTIONS

ACCESS TO
 1M NaOH
 1M NH 4OH
 1M HCL
 0.01m PB (NO 3) 2
 Source of heat
 PH chart (PH=1 to 14)
 10ml of solution K
 Sodium hydrogen carbonate
Question 1.
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1. Solution J 100cm
2. Burette
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3. Solution K100cm
4. Pipette
5. 2 conical flasks
6. Filter funnel
7. Retort stand

PREPARATION OF SOLUTIONS
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1. Solution J - Dissolve 17g of ammonium iron (ii) sulphate in 50cm of 2M H 2SO 4 dilute to 1dm
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2. Solution K-KMnO 4 - Dissolve 1.6g of potassium manganate vii in 20cm of 2 MH 2SO 4 dilute to 1dm
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3. Solution R - Dissolve 40g of sodium thiosulphate in 1dm of solution
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4. Solution S - Dissolve 172cm of concentrated hydrochloric acid in 1dm of solution
5. Solid Y is aluminium sulphate
6. Solid Z is oxalic acid.

1. You are provided with:
 Solution M 1 aqueous solution of a monobasic acid, HB containing 1.62425, of the acid
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dissolve in 250cm of the solution
 0.208M sodium hydroxide solution.
You are required to determine
a) The molarity of the acid
b) The RFM of the acid and the RAM of B in HB (H=1, C=12, O=16)
Procedure
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Pipette 25cm of solution M1 into a clean dry conical flask. Add 2 drops of phenolphthalein
indicators. Fill the burette with solution Q and titrate against solution M 1
Repeat the procedure two more times and complete the table below:
I II III
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Final burette reading(cm )
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Initial burette(cm )
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Volume of solution Q used (cm )

a) Determine the average volume of solution Q used
b) Write an equation for the reaction between solution M 1 and Q
c) Calculate:
i) The number of moles of Q used
ii) The number of moles of M 1 used
iii) The molarity of solution M 1
d) Determine;
i) The RFM of acid
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