Page 45 - PIGNAT catalogue 2020 GB_092020

OTP PILOTS

OTP-RPI 50 L MULTI-PURPOSE STAINLESS STEEL REACTOR

➢ Carry out operations of fine chemistry product synthesis

Perform and study reactions
Esterification or saponification
Concentration by evaporation
Crystallization by cooling

Knowledge of reaction's characteristics
Basic, aqueous, organic, mineral medium
Endo or exothermic reaction
Bi-phase catalytic reaction

Carrying out of an operation depending on operating conditions
Working pressure: atmospheric or vacuum
Monitoring of cooling during crystallization
Management of the distillation with reflux ratio definition

General specifications Instrumentation
• Vacuum gauge.
• SS conical tank, double jacket and insulated. • Gauge.
• Liquid column manometer.
• Stirrer, SS mobile and shaft. • 6 temperature probes Pt100Ω.
www.pignat.com

• 2 gas expansion thermometer for reactor
www.pignat.com -SS büchner filter.
• Feeding funnel, SURLYN coated.
and vent.

• 6 flowmeters
• Column, packed with glass Raschig rings.
Option

• Partial condenser, SS shell and tubes.

• Total condenser.

• Decanter, double jacket, vacuum connec-
tion, overflow tube.

200 - 400 V Water 20 kg/h 1000 Drainage
3ϕ - 50/60 Hz 1000 L / h 6 bar max mbar
absolute

Dim: 170 x 160 x 450 cm - 200 kg

TI2
Conical reactor, capacity of 50L, RPI OTP allowed the chemical synthe- TI5 TI6
sis realization in industrial conditions. The suction system allows filling 8
of the funnel 4. Vapeur calorifugée S=0.9m2 S=0.9m2 TI8
TI1 6 Alimentation eau de refroidissement
A manifold allows the double jacket steam feeding 17 or the cold
water feeding 15.
7 9 monte jus
A spotlight allows to visualize the reaction mixture at any time. 17 5 4
11 Vide
A venting system allows to put the receivers at atmospheric pressure 3 DP 10
for the draining during a workshop. M 12
O1 14 TI4 16
monte jus TI7 PI1 1
Variant UPR/1510 PI3 15
(page 36) TI3
13
2

Option

Steam generator.
empotage

Chemical engineering & unit operations 45