Page 361 - Pharmacognosy 2 PG303
P. 361

Constituents        Pharmacognosy-2 (PG303)

                     yellow crystalline anthraquinone glyco
                     barbaloin, resin, aloe-emodin (hydroly
                     decomposition product of barbaloin).

Uses                • Purgative (used in constipation as
Tests for Identity      digestion and does not lose its act
                        repetition).

                    • treatment of burns, skin irritations
                        effects

                    0.5 g powder + 50 ml water → boil for 2-3 mi
                    kieselguhr → shake and filter
                    → clear filtrate, the clear filtrate responds to
                    identification:

                    1-Borax test for anthranols:

                    0.2 g borax + 5 mL filtrate → Dissolve by hea
                    drops of this solution to a test tube nearly fille

                    green fluorescence Is produced due to
                    aloe-emodin anthranol liberated from

                    hydrolysis with borax

                    2- Test for free anthraquinones:

                    10 mL filtrate + 20 mL ether → shake 10 mL
                    mL of diluted Soln
                    of NH4OH

                    A rose red color is produced in ammo
                    3- Test for barbaloin (Bromine wate

                    1 mL filtrate + 1 mL bromine T.S

                    pale yellow ppt. is formed
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