Page 18 - Fuel Cell Student Edition
P. 18

7.  Wrap the long bare end around the bottom of
                                                                    the 5mL tube  between the start  of  the cone
                                                                    and the 1mL mark.

                                                                 8.  Bend the wire toward the top of the tube and
                                                                    secure it with electrical tape. Do not cover the
                                                                    bare end of the wire with tape

                                                                 9.  Measure out 20mL of  NaOH solution. The
                                                                    white material surrounding the cap is sodium
                                                                    carbonate. It is a byproduct of the NaOH solution
                                                                    reacting with CO  in the air space at the top of
                                                                                    2
                                                                    the bottle. Pour 10mL of the NaOH electrolyte
                                                                    solution into the  carbon bottle slowly. When
                                                                    the carbon bubbling slows, pour in the other
                                                                    half to make a total dispensed volume of 20mL.






             LAB PROCEDURE                                           WARNING!
                                                                     NaOH is extremely caustic! It will burn
             1.  Fold the Zinc strip to fit in the 5mL tube below    your skin within minutes of exposure
                 the 4 mL mark.                                      and may cause permanent blindness,
                                                                     even at low concentrations. Wear eye
             2.  Cut a piece of wire 140mm (5.5”). Strip one         protection and gloves until the fuel cell
                 end  back 12mm (½”). Strip  the other end           is sealed in step 11. If you are exposed
                 50mm (2”).                                          to NaOH, immediately flush the
                                                                     affected area with large quantities of
             3.  Wrap the longer bare end of the wire around the     water and alert your instructor.
                 end of the zinc strip a few times until the wire
                 insulation is touching the zinc strip.

             4.  Place the zinc  strip/wire  assembly into  the   10. With the blue cap end facing up, insert the
                 5mL tube.                                          5mL tube  assembly into the  bottle until it is
                                                                    resting on the bottom of the bottle. You may
             5.  Thread the wire through the cap and screw          press the tube gently down to get it into place,
                 the cap onto the tube. Push the wire down to       but try not to push hard enough to disrupt
                 ensure that the zinc is at the bottom of the       the coil of wire surrounding the tube.
                 tube.
                                                                 11.  Wrap a length of electrical tape tightly around
             6.  Cut a piece of wire 215mm (8.5”) long and          the top of the entire fuel cell assembly to keep
                 strip one end back 12mm (½”). Strip the other      it from leaking if it accidentally gets tipped
                 end 95mm (3.75”).                                  over.








              18   TOTAL REDOX™ – FUEL CELLS                                                                                                                                                                 TOTAL REDOX™ – FUEL CELLS   19
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