Page 36 - PIGNAT catalogue 2020 GB_092020

REACTION - SYNTHESIS

UPR/1510 MULTI-PURPOSE MANUAL REACTOR—STEAM HEATING

➢ Multipurpose unit for :
Liquid-liquid mixture
Solid-Liquid dissolution
Evaporation, concentration
Reaction, synthesis
Distillation
Decantation, crystallization

➢ Heating by steam generator

➢ Cooling by water circulation inside the double
jacket
Operator training to monitor the process
Unit placed under vacuum
Compliance with procedures
Loading through the dropping funnel
Receivers draining under vacuum
Phenomena viewing
Synoptic follow
Curves using
Unit cleaning
Follow - up of reaction kinetics
www.pignat.com Kinetic, material balance, reaction yield
www.pignat.com Handling report

Separation of the products

By distillation, decantation or crystallization

General specifications

Supervision - Data acquisition • Jacketed SS vessel. SS flat cover. • Cold water circuit.
• Steam circuit: with solenoid valve,
insulated pipes.
• Variable speed stirrer.

• Glass feeding vessel. Instrumentation
• 5 temperature probes Pt100Ω.
• Glass distillation column, SS Multiknit • 3 flowmeters flow detector.
packing. • Vacuum manometer.
• Solenoid valve on steam circuit.
• Reflux divider with PTFE pneumatic valve.

• Glass calendar condenser and SS coil. Safety
• Discharge check valve.
• Glass azeotropic decanter, glass double • Motor coupling and reactor protection.
jacket. • Steam cut off in case of emergency.

Option • SS distillate cooler.

Steam generator.
• Two graduated glass receivers, three
ways selecting valve, setting, vent and
draining valves.

Exist in OTP version • Vacuum circuit with vacuum trap.
(page 45) 200 - 400 V Water 6 bar max
1ϕ/3ϕ - 50/60 Hz
• Vacuum pump.
Dim: 190 x 75 x 255 cm - 350 kg
Dim steam generator: 60 x 70 x 80 cm—78 kg

36 Chemical engineering & unit operations