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Suguna Management System      Ver 1.0 / SOP / FQL / P1 - 06   Page  1 of 2



























           6. Laboratory Glassware Cleaning Procedure


                                                                   FIt  is  corrosive  to  equipment.  It  is  rather
           SCOPE
                                                                       difficult  to  remove  completely  by  rinsing
           This standard operational procedure applies to all          with water; unknowingly it may enter into
           laboratory glassware used during the production             the  analysis  serious  analytical  errors,
           of laboratory reagents and/or the preparation of            particularly while determining K, Na or SO
           samples.                                                                                             4
                                                                       chromic acid mixture not is used.

           EQUIPMENT
                                                                2.  General Laboratory Glassware
           FGlassware dishwasher
                                                                FObjects  that  are  too  large  to  be  washed
           FDeionised water purification system                    effectively in the washer, should be soaked in a
                                                                   10% detergent (Contra NF or similar) bath.
           FLarge capacity drying oven 75 °C
                                                                FUse  acetone  to  remove  any  writing  on  the
           FLarge capacity drying oven 110 °C                      glassware.

                                                                FRinse thoroughly with tap water, ensuring there
           COMMON CLEANING AGENTS
                                                                   are not any particles left on the glassware that
           1.  Preparation of chromic -acid mixture
                                                                   may clog the washer.
           FIt  can  be  prepared  by  adding  360  ml  of
                                                                FLoad  in  washer  so  that  each  piece  will  be
              concentrated  H SO   with  580  ml  cooled
                               2
                                   4
              distilled water in the   side ways. After 3 hours    washed  and  rinsed  properly  and  Start  the
              add  60g  of  potassium  dichromate  to  this        washer.
              solution and stir well. Before using it can be    FAfter  the  wash  cycle  is  complete,  allow  the
              made up to 5 litres.                                 glassware  to  cool  and  put  them  in  the
                                                                   appropriate oven.
           FChromic acid mixture should not be used till it is
              needed for some purposes because:                 FPut glassware in the 110 °C oven and plastic
                                                                   ware  in  the  75°C  oven.  Glassware  that
              FIt  is  dangerous,  especially  when  hot,  if
                 spilled or spattered on skin or clothing.         contains rubber seals (i.e. blender jars) should




          Prepared by :                                                             Approved by :
                                                             27                                    Director - Technical
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