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Laboratory Glassware Cleaning Procedure       Suguna Management System      Ver 1.0 / SOP / FQL / P1 - 06  Page  2 of 2


              be dried in the 75 °C oven.                       making the acid bath.

                                                                SAFETY  NOTE:  Put  on  protective  equipment
           3. Mycotoxin Glassware
                                                                before working with the 10% HNO  solution bath.
                                                                                                  3
           FUse  acetone  to  remove  any  writing  on  the     You  should  have  on  protective  gloves,  a  face
              glassware.
                                                                shield and an apron or lab coat.
           FRinse thoroughly with tap water, ensuring there     FUse  acetone  to  remove  any  writing  on  the
              are not any particles left on the glassware that
                                                                   glassware.
              may clog the washer.
                                                                FRinse  the  glassware  as  well  as  possible  to
           FLoad  in  washer  so  that  each  piece  will  be
                                                                   avoid contamination of the 10% HNO  solution
              washed and rinsed properly.                                                               3
                                                                   bath.
           FStart the washer. Allow the washer to flush for
                                                                FMake  sure  the  glassware  is  completely
              approximately 3 minutes and then fill with water
                                                                   submerged in the bath and allow it to soak for
              and add 350 ml of detergent (DRI-CONTRAD
                                                                   at least two hours.
              or similar) to the wash.
                                                                FCarefully remove the glassware from the bath,
           FClose the washer door and press start on the
                                                                   making sure not to splash the acidic solution
              control panel.
                                                                   on you.
           FAfter  the  wash  cycle  is  complete,  allow  the
                                                                FRinse thoroughly with deionised water.
              glassware  to  cool  and  put  them  in  the
              appropriate oven.                                 FPut glassware in the 110 °C oven and plastic
                                                                   ware  in  the  75°C  oven.  Glassware  that
           FPut glassware in the 110 °C oven and plastic
                                                                   contains rubber seals (i.e. blender jars) should
              ware  in  the  75°C  oven.  Glassware  that
              contains rubber seals (i.e. blender jars) should     be dried in the 75 °C oven.
              be dried in the 75 °C oven.



           4.Cleaning  Procedures  Using  Baths/Tubs
              (Nitric Acid Bath, 10%)
           All glassware used in mineral methods must be
           cleaned using a 10% HNO  solution bath. Only
                                       3
           Trace Metal grade HNO  should be used when
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          Prepared by :                                                             Approved by :
                                                             28                                    Director - Technical
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