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th
                               8  Biannual Conference on Chemistry - CHEM 08

                      3D Porous Catalysts: Noble Metal-free Foams Prepared by

                              DHBT for Efficient Glycerol Electro-oxidation

                            Mohamed R. Rizk*, Muhammad G. Abd El-Moghny, Amina
                                            Mazhar, Mohamed. S. El-deab
                         Chemistry department, Faculty of Science, Cairo University, Cairo,
                                                          Egypt
                                              Email: mkhater@sci.cu.edu.eg

                                                       ABSTRACT

                        Three-dimensional macroporous  noble metal-free films are
                        successfully prepared by one step electro-deposition via hydrogen
                        bubbles dynamic templates (DHBT) method. The prepared films are
                        characterized by scanning electron microscope (SEM), electron
                        dispersive X-ray (EDX), X-ray diffraction (XRD), and  X-ray
                        photoelectron spectroscopy (XPS). Moreover, the prepared electrodes
                        are found to have high mechanical stability and electrochemical
                        activity towards glycerol electro-oxidation and water splitting in
                        alkaline medium.
































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