Page 26 - PIGNAT catalogue 2020 GB_092020
P. 26

LIQUID-LIQUID EXTRACTION





          ELA/2000  STIRRED LIQUID-LIQUID EXTRACTION


                                                             ➢     Liquid - Liquid extraction in a stirred column


                                                             Study of a continuous liquid-liquid extraction
                                                                   Process parameters
                                                                   Interphase level determination

                                                             Ternary diagram
                                                                   Mass balance
                                                                   Column effiency determination (HUT/NUT)




                                                                  General specifications   •  Inter-phase  level  setting  by  lateral
                                                                                          crosshead.
                                                             •  2 SS/PEEK pumps.
                                                                                        •  4 sampling valves.
                                                             •  Glass  decanter  with  light  phase
                                                               outlet, heavy phase feeding.   •  Polyethylene storage tank, 10 L.

                                                             •  Glass column.                  Instrumentation
                                                               •  Stirring   shaft,   made   of   SS    •  2 flowmeters.
                                                    www.pignat.com
                                                  www.pignat.com                           Dim: 140 x 60 x 240 cm  -  120 kg
                                                               Rushton type stirrer.

                                                             •  Glass  decanter  with  heavy  phase
                                                                                                   100  - 240 V
                                                                                                           Ventilation
                                                               outlet, light phase feeding.
                                                                                                  1ϕ - 50/60 Hz







                                                                                     9


                                                                                         7
                                                                              11






                                                                 3        6
                                                                                    8
               Liquid-liquid extraction is a fundamental material transfer
               operation  based  on  the  varying  solubility  of  the
               components of a mixture. It entails extracting a compound
               from a solution (solute dissolved in a diluent) by selective   PE  PE         PE          PE
               transfer to a second liquid (solvent), non-miscible with the                        0,5 L      0,5 L
               first and with different density.              2    P1  5   P2           10
                                                                                                  12          13
               A stirring device 9,  allows to stir the liquid in the column,
               increasing  the  contact  between  the  two  phases  and  the
               mass transfer from one to another.
                                                                1       4
                                                                                                10 L        10 L
                                                                10 L     10 L




        26                                                            Chemical engineering & unit operations
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