Page 321 - SUBSEC October 2017_Neat
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UNIT 2
               MODULE 2: ANALYTICAL METHODS AND SEPARATION TECHNIQUES (cont’d)


                SPECIFIC OBJECTIVES                 EXPLANATORY NOTES            SUGGESTED PRACTICAL
                                                                                 ACTIVITIES

                Phase Separations cont’d

                Students should be able to:

                9.3.     discuss   the    chemical   Laboratory  work  on  the
                         principles and use of steam   extraction  of  essential  oils
                         distillation;               from    plant   materials.
                                                     Purification          of
                                                     nitrobenzene         and
                                                     phenylamine.      Simple
                                                     calculations are required.

                9.4.     discuss the principles upon   A  discussion  on  partition
                         which  solvent  extraction  is   coefficient   and   simple
                         based;                      calculations are required.

                9.5.     select appropriate methods                             Conduct simple separation
                         of  separation,  given  the                            experiments   based   on
                         physical   and   chemical                              solute         partitioning
                         properties    of      the                              between  two  immiscible
                         components of a mixture;                               solvents.   These   could
                                                                                include  the  separation  of
                                                                                an acid/base mixture.

                9.6.     perform        distillation   These  should  include  (but
                         experiments; and,           not  be  limited  to)  a
                                                     comparison     of    the
                                                     efficiency of separation of
                                                     ethanol in beer or rum by
                                                     simple   and    fractional
                                                     distillation.

                9.7.     cite   examples  of   the   Include  petroleum,  rum
                         applications   of     the   and     the     fragrance
                         distillation methods used in   industries.
                         various industries.














                          CXC A11/U2/17                    52
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