Page 316 - SUBSEC October 2017_Neat
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UNIT 2
               MODULE 2: ANALYTICAL METHODS AND SEPARATION TECHNIQUES (cont’d)


                SPECIFIC OBJECTIVES                  EXPLANATORY NOTES           SUGGESTED PRACTICAL
                                                                                 ACTIVITIES

                3.        Gravimetric Methods of Analysis

                Students should be able to:

                3.1.     explain  the  principles  upon   Limited to  a discussion on
                         which  gravimetric  analyses   precipitation     and
                         are based;                  volatilisation methods.

                3.2.     describe  the  functions  of   Limited  to  suction  flasks,
                         the  various  pieces  of basic   suction   funnels,   silica
                         equipment     used     in   crucibles,   sinter   glass
                         gravimetric analyses;       crucibles  and  ovens  and
                                                     furnaces.

                3.3.     perform experiments based                              Limited       to
                         on            gravimetric                              experiments      involving
                         determinations;                                        volatilisation   methods,
                                                                                such  as,  moisture  content
                                                                                of    soils;   water   of
                                                                                crystallisation.

                3.4.     perform  calculations  based   Use  data  from  actual
                         on  data  obtained  from    experiments carried out
                         gravimetric analyses; and,   or from the literature.

                3.5.     cite examples of the use of   Examples        include
                         gravimetric   analysis   in   determination of SO2 in the
                         quality control.            air,  in  wine  or  fruit  drink;
                                                     determination   of   the
                                                     amount  of  elements  such
                                                     as    phosphorous      in
                                                     fertilizers; the chloride ion
                                                     presence in water supply.

                4.        Spectroscopic Methods of Analysis

                Students should be able to:

                4.1.     explain  the  nature  of    Calculations   using   the
                         electromagnetic radiation;   equation:

                                                     E = hv = hc/λ are required.





                          CXC A11/U2/17                    47
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