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UNIT 2
               MODULE 2: ANALYTICAL METHODS AND SEPARATION TECHNIQUES (cont’d)


                SPECIFIC OBJECTIVES                  EXPLANATORY NOTES           SUGGESTED PRACTICAL
                                                                                 ACTIVITIES

                Uncertainty in Measurements cont’d

                Students should be able to:

                1.3.     select appropriate pieces of   Selection  of  equipment
                         equipment     to    make    limited to those in Specific
                         measurements,  depending    Objective 1.2 above.
                         upon    the   degree   of
                         accuracy required.


                2.        Titrimetric (Volumetric) Methods of Analysis

                Students should be able to:

                2.1.     explain  the  basic  principles
                         upon   which    titrimetric
                         analyses are based;

                2.2.     discuss  the  criteria  used in   NaHCO 3 ,  Na 2 CO 3 ,  KIO 3,
                         selecting primary standards;   (COOH) 2  and  its  salts  as
                                                     primary standards.

                                                     Definition   of   primary
                                                     standards required.

                2.3.     use  data  obtained  from
                         potentiometric
                         thermometric         and
                         conductrimetric   methods
                         for  titration  which  do  not
                         require   the   use    of
                         indicators;

                2.4.     perform experiments based                               Experiments  should  be
                         on titrimetric analyses;                                limited  to  acid-base,  back
                                                                                 and        redox        titrations.
                                                                                 Include   preparation   of
                                                                                 standard solutions.

                2.5.     perform  calculations  based   Refer to Unit 1,  Module 2,
                         on  data  obtained  from    Specific Objective 3.6.
                         titrimetric  analyses; and,

                2.6.     cite examples of the use of   Refer   to     vinegar,
                         titrimetric  analysis  in  the   household   cleaners,
                         quantification  of  various   vitamin  C  tablets,  aspirin,
                         substances.                 antacids.



                          CXC A11/U2/17                    46
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