Page 15 - ST Sept
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METALWORKING EQUIPMENT                                                          METALWORKING EQUIPMENT
 AND TOOLS                                                                       AND TOOLS
 and copper, which is in the pseudo-alloy in an unbound state, passes from the roller into a solid      Samples with coatings based on Ti-Al-N
 solution of austenite.                                       and Mo-Cr-N were manufactured at OOO NPF
    Upon  cooling,  the  austenite  solution is supersaturated  with tungsten,  and  the  excess   Plazmacer (St. Petersburg). Comparative tests
 tungsten precipitates in the form of a tungsten carbide network (Fig. 2) along the boundaries of   of  the wear resistance  of  the  samples  were
 austenite grains lightly alloyed with tungsten. In this case, the resulting structure is identical to   carried out on an automated installation based
 the structure of cast high speed steel, corresponding to a complex carbide eutectic, reminiscent   on  the  MI-1M  friction  machine  designed  for
 of ledeburite and located along the grain boundaries. Vickers microhardness was measured on   tribotechnical tests  of  cylindrical specimens
 a microhardness meter mod. PMT-3M with a load of 200 gr. The measurement of the diagonals   made of metallic materials and alloys, allowing
 of the prints was carried out using an inverted metallographic microscope Metam LV-34 using   to determine  the  tribotechnical indicators of
 the automated analysis system "Micro-Analysis View".         surfaces  in conditions of  sliding  friction  with
    Table 4 shows the values of Vickers microhardness for a multi-layer hardened gradient   boundary  lubrication using the  normalized
 structure of a wear-resistant surface (Fig. 1). Table 5 shows the data on the hardness of steel   method [5].
 R18. Comparison of the data on hardness                              During  tests  with  a  specified  load  and
 shows that in fact the surface layer of 45                   sliding speed, a stationary cylindrical indenter
 carbon steel is a gradient structure of tool   Fig. 2. Microstructure of layer 1 (tungsten carbide particles)   was  pressed  against  the  rotating  cylindrical
 steel R18. To determine the wear resistance   and layer 2 (tungsten carbide mesh along the boundaries of   surface  of  the  sample  partially immersed in
 of a typical inexpensive structural 45 steel    austenite grains.
 with a gradient structure of the hardened   the  lubricant.  To  install the  samples  and  the
 surface, comprehensive comparative tests   indenter,  a  scheme  with replaceable  holders
 of the wear resistance of rather expensive   was  used,  which provides  self-alignment  of
 and  technologically  difficult  to  obtain   the indenter relative to the test surface of the
 modern wear-resistant coatings.  sample  on  an  intermediate  spherical  support
    The  tribotechnical  indicators  of  the   for  the  implementation  of  a  linear  contact.
 outer cylindrical surfaces of samples made   During  the  tests,  using  a  system  of  sensors,
 of  steels R18 and  45  using the  following   the test time, load, coefficient of friction and
 technologies were examined:  linear  wear  were  recorded  continuously  and
    synchronously.  Their numerical  values  were
    displayed  on  a  personal  computer  monitor.
    To measure the moment of friction and load,
    strain gauges  were  used.  For  continuous
 Fig. 1. Surface structure of a steel sample hardened with tungsten   measurement of wear during testing, a special
 carbide.  circuit was  developed  with the  use  of  an        Fig. 3. Results of tests of a sample of R18 steel after
    inductive  sensor, which makes  it possible to              volumetric quenching and low-temperature tempering.
 Table 3.  exclude the influence of the radial runout and
 Energy dispersive analysis (Fig. 2), mass. %.  thermal deformations of the test specimen on the measurement results.
            According  to  the  results  of  the  analysis  of  the  registered  parameters,  the  following
 points  c  Al  Fe  Cr  Cu  W  total  indicators of tribotechnical properties were determined:
 1  16,8  -  4,0  -  -  79,2  100,0     ● running-in time t0, h, defined as the time from the start of the test to the time when
 2  7,6  -  6,4  14,7  -  71,3  100,0  the wear curve reaches the normal wear area;

 3  3,3  -  84,2  -  2,9  9,6  100,0
 4  3,6  -  83,6  -  2,7  10,1  100,0
 5  15,1  0,6  71,5  -  4,0  8,8  100,0  Table 4.
 6  11,8  0,7  76,9  -  2,1  8,5  100,0  Microhardness of the surface layer of 45 steel, hardened with tungsten carbide.
 7  11,3  0,6  88,1  -  -  -  100,0           Microhardness of HV layer
                layer 1                      layer 2                     layer 3                     matrix

    ● volumetric hardening, low-temperature tempering (R18 steel);  741…846  546…633  431…525      304…332
    ● volumetric hardening, low-temperature tempering (R18 steel) + a coating with solid
 solution hardening from compounds with different types of interatomic bonds of the Ti-Al-N   Table 5.
 system  with a thickness of  3 microns,  applied using PVD  technology  (in vacuum  using an   The hardness of steel R18 in the heat-treated state at elevated temperatures
 electric arc plasma source and separation of a plasma flow) ;  Test temperature ºC  HV     HRC
    ● volumetric hardening, low-temperature tempering (R18 steel) + coating with a multiphase   200  815  64
 structure of the Mo-Cr-N system with a thickness of 3 microns, applied using PVD technology   400  755  62
 (in vacuum using an electric arc plasma source and plasma flow separation);  500  712       60
    ● combined electromechanical treatment (CEMT) the formation of a surface layer implanted   550  661  58
 with tungsten carbides on the surface of untreated 45  steel and subsequent electromechanical   600  615  56
 hardening of the treated surface.  650                     504                              51

 14  Stanochniy park                                                                            Stanochniy park      15
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