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Suguna Management System      Ver 1.0 / SOP / FQL / P2 - 42  Page  1 of 1























           42. Estimation of sodium bicarbonate assay







           SCOPE                                                REAGENTS
           The estimate of purity for Sodium bicarbonate        F0.5N  H SO   -  13.6  ml  of  Con.Sulphuric  acid  in
                                                                              4
                                                                          2
                                                                   1000 ml of distilled water.
           INTRODUCTION
                                                                FMethyl orange indicator solution
           It  is  white  crystalline  powder  or  small,  opaque
           monoclinic crystals. It is odour less and saline in taste. It
                                                                PROCEDURE
           is freely soluble in water, partially insoluble in alcohol
                                                                1. Weigh accurately about 1.0g of sample in 250ml
                                                                   conical flask
           APPARATUS
           FConical Flask 250ml                                 2. Add  20  ml  of  distilled  water    and  few  drops  of
                                                                   Methyl orange indicator
           FBurette, 10ml
                                                                3. Then titrate with 0.5 N  H SO .
                                                                                         2   4
                                                                Note: Each ml of 0.5 N  H SO  is equivalent to 0.042 g
                                                                                       2
                                                                                           4
                                                                of NaHCO .
                                                                         3

           CALCULATION

                                                                TV X N.of H SO  X 0.042 X 100
                                                                2
                                                                   4
                             SBC Purity % = ------------------------------------------------------------
                                                                       Sample Weight, g

















          Prepared by :                                                             Approved by :
                                                            119                                    Director - Technical
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