Page 55 - Feed Lab

NIR Analysis Procedure Suguna Management System Ver 1.0 / SOP / FQL / P1 - 10 Page 2 of 3

of major and minor sample PROCEDURE FOR CHECK CELL
components; ANALYSIS BY NIR SYSTEM

b) Seasonal, geographic and genetic
From the Opening menu
effects on forages, feed raw material
and cereals;
Click on Analysis
c) Processing techniques and conditions;

d) Storage conditions; and
Highlight Scan Samples and Click
e) Sample and instrument temperature.

FCalibrations must be provided with statistical Press Enter
information on its performance such as
number and type of samples, correlation,
standard error of calibration and prediction and Highlight on Check Cel
in a format that allows for the identification of
outliers.
Highlight on Check Cel
Reference Analyses and NIR measurements
FInternationally accepted reference methods for Press Enter
determination of moisture, fat, protein and
other constituents and parameters should be
used. Highlight on Analyze Check Cell

FThe reference method used for calibration
should be in statistical control, i.e. for any Press Enter
sample, the variability should consist of
random variations of a reproducible system. It
is essential to know the precision of the The Check Cell Scanning
Starts and after a few Minutes
reference method. it will be completed

Highlight on Standard Check Cell

Note :
Press Enter
The Check cell should be scanned daily and before
F
Scanning the Equipment it should be kept in
Analysis mode at least for 30 mins.
Result will be displayed
FOn the instrument check the Check cell
performance after analysis unknown sample.
Press Enter
FMonthly basis analyse the Diagnostics. And check
the Performance of Accuracy & Repeatability of the
NIR Instrument.

Prepared by : Approved by :
45 Director - Technical