Page 171 - Chem Service 2016 Catalogue
P. 171

METHOD 632 - CARBAMATE UREA PESTICIDES

          Method 632 is applicable to the determination of carbamate and urea pesticides in industrial and municipal wastewater by high performance
          liquid chromatography (HPLC).  Note that this method provides for an optional Florisil column cleanup procedure, to aid in the elimination or
          reduction of interferences, which may be encountered (caused by contaminants in solvents, reagents, glassware and other sample processing
     EPA 600  CARBAMATE & UREA PESTICIDES MIXTURE
          apparatus that lead to discrete artifacts or elevated baselines in liquid chromatograms).

         EPA METHOD 632
         Aminocarb


                                                                             Oxamyl
         Barban                                        Fenuron               Neburon

                                                    Fluometuron
         Chlorpropham                               Linuron                  Propoxur
         Carbaryl                                   Methiocarb               Siduron
         Carbofuran                                  Methomyl                Diuron
         Monuron                                    Swep                     Propham
         1000ug/mL in Acetonitrile          (18 components)
         M-CUP6321A4-1ML            1mL Ampule
         CARBAMATE & UREA PESTICIDES MIXTURE
         EPA METHOD 632
         Aminocarb             Diuron                 Methomyl                Propoxur
         Barban                Fenuron              Monuron                  Siduron
         Carbaryl              Fluometuron          Neburon                  Swep
         Carbofuran            Linuron              Oxamyl                   Zectran (Mexacarbate)
         Chlorpropham          Methiocarb           Propham

         1000ug/mL in Acetonitrile          (19 components)
         M-CUP6322A4-1ML            1mL Ampule

         ADDITIONAL ANALYTES
         EPA METHOD 632
         N-11968-1G        Fenuron TCA
         N-12498-100MG     Monuron TCA
            METHOD 634 - THIOCARBAMATE PESTICIDES
          Method 634 is applicable to the determination of thiocarbamate pesticides in industrial and municipal wastewaters.  Sample extraction
          and concentration steps in this method are similar to other 600 Series Methods.  The separation and measurement of the compounds in the
          extract is by alkali flame detector (AFD) gas chromatography.  To aid in the elimination of interferences an optional silica gel column cleanup
          procedure is provided. This method describes analytical conditions for a second gas chromatographic column that can be used to confirm
          measurements made with the primary column, as well as the gas chromatograph/mass spectrometer (GC/MS) criteria appropriate for the
          qualitative confirmation of these compound.
         THIOCARBAMATE PESTICIDES MIXTURE                      INTERNAL STANDARDS
         EPA METHOD 634                                        EPA METHOD 634
         Butylate                                              N-13708-1G      Triphenyl phosphate
         Cycloate                                              S-13708T3-1ML   500ug/ml in t-Butylmethyl ether
         S-Ethyl dipropylthiocarbamate                         S-13708T3-5ML   500ug/ml in t-Butylmethyl ether
         Molinate                                              SURROGATE STANDARDS
         S-Propyl butylethylthiocarbamate
         Vernolate                                             EPA METHOD 634
                                                               N-10114-1G       1,3-Dimethyl-2-nitrobenzene
         1000ug/mL in tert-Butylmethyl ether   (6 components)  S-10114T6-1ML    2500ug/ml in tert-butylmethyl ether
         M-TCP507T4-1ML                     1mL Ampule         S-10114T6-5ML    2500ug/ml in tert-butylmethyl ether
                                                               S-10114T5-1ML    2000ug/ml in tert-butylmethyl ether
                                                               S-10114T5-5ML    2000ug/ml in tert-butylmethyl ether
            METHOD 635 - ROTENONE

          Method 635 is applicable to the determination of rotenone (as well as separation and measurement of the compounds in the extract by HPLC/
          UV) in industrial and municipal wastewaters.
         ROTENONE STANDARDS
         EPA METHOD 635
         N-13184-250MG   Rotenone
         S-13184X4-1ML     1000ug/ml in Methylene chloride
         S-13184X4-5ML     1000ug/ml in Methylene chloride








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