Page 173 - Chem Service 2016 Catalogue
P. 173

METHOD 644 - PICLORAM

          Method 644 is applicable to the determination of Picloram in municipal and industrial wastewater by extraction, followed by analysis by HPLC
          with ultraviolet (UV) detection. An alkaline back-extraction is used as necessary to eliminate interferences.
     EPA 600  EPA METHOD 644                                   EPA METHOD 644
         PICLORAM STANDARDS
                                                               INTERNAL STANDARDS
         N-13050-250MG  Picloram
                                                               N-13200-1G
                                                                                Salicylic acid
         S-13050A4-1ML   1000ug/ml in Acetonitrile
                                                               S-13200L5-1ML    2000ug/ml in Isopropanol
         S-13050A4-5ML   1000ug/ml in Acetonitrile
         S-13050B1-1ML    100ug/ml in Acetone
         S-13050B1-5ML    100ug/ml in Acetone                  S-13200L5-5ML    2000ug/ml in Isopropanol
            METHOD 645 - AMINE PESTICIDES & LETHANE
          Method 645 is applicable to the determination of amine pesticides and Lethane in municipal and industrial wastewater.  Analysis is by
          gas chromatography.  Measurement of the pesticides is accomplished with a nitrogen/phosphorous specific detector. This method provides
          identification by gas chromatography/mass spectrometer (GC/MS).
                                                               INTERNAL STANDARDS
         INTERNAL STANDARDS                                    EPA METHOD 644
         EPA METHOD 645                                        N-13200-1G       Salicylic acid
         N-13708-1G        Triphenyl phosphate                 S-13200L5-1ML    2000ug/ml in Isopropanol
         S-13708T3-1ML    500ug/ml in t-Butylmethyl ether      S-13200L5-5ML    2000ug/ml in Isopropanol
         S-13708T3-5ML    500ug/ml in t-Butylmethyl ether
            METHOD 680 - PESTICIDE & PCB CONGENERS

          Method 680 is applicable to the determination of pesticides and PCB congeners by gas chromatography and mass spectrometry.
         ORGANOCHLORINE PESTICIDES MIXTURE #1
         EPA METHOD 680, 508, 508.1, 525.2, 608, 617, 625, 8080A/8081, 8250A/8270B, CLP
         Aldrin (TM)                      b-Endosulfan             BHC (alpha isomer)           BHC (beta isomer)
         BHC (delta isomer)               cis-Chlordane            4,4’-DDD                     4,4’-DDE
         4,4’-DDT                         Dieldrin                 a-Endosulfan                 Endosulfan sulfate
         Endrin                           Endrin aldehyde          Endrin ketone                Heptachlor
         Heptachlor epoxide (Isomer B)    Lindane (BHC gamma isomer)   Methoxychlor             trans-Chlordane
         1000ug/mL in tert-Butyl methyl ehter    (20 components)
         M-OCP5081T4-1ML                      1mL Ampule

                                                               INTERNAL STANDARDS
                                                               EPA METHOD 680
         TUNING STANDARDS                                      N-11467-10MG     Chrysene-d
                                                                                        12
         EPA METHOD 680                                        S-11467X5-1ML     2000ug/mL in Methylene chloride
         N-11571-10MG      Decafluorotriphenylphosphine        S-11467X5-5ML      2000ug/mL in Methylene chloride
         S-11571BO-1ML     50ug/ml in Acetone                  N-12856-100MG     Phenanthrene-d
         S-11571B0-5ML     50ug/ml in Acetone                  S-12856M1-1ML     100ug/mL in Methanol
                                                                                           10
         S-11571X0-1ML     50ug/ml in Methylene Chloride       S-12856M1-5ML     100ug/mL in Methanol
         S-11571X5-1ML     2000ug/ml in Methylene chloride     S-12856X5-1ML     2000ug/mL in Methylene chloride
                                                               S-12856X5-5ML     2000ug/mL in Methylene chloride
         PCB CONGENER MIXTURE #1
         EPA METHOD 680
         50µg/mL        2,4,5-Trichlorobiphenyl        50 µg/mL       2,3-Dichlorobiphenyl
         250µg/mL       Decachlorobiphenyl          50µg/mL           2-Chlorobiphenyl
         100µg/mL       2,2’,3,4,5’-Pentachlorobiphenyl      150 µg/mL      2,2’,3,3’,4,5’,6,6’-Octachlorobiphenyl
         100 µg/mL      2,2’,4,4’,5,6’-Hexachlorobiphenyl     100 µg/mL      2,2’,4,6-Tetrachlorobiphenyl
         150 µg/mL      2,2’,3,4’,5,6,6’-Heptachlorobiphenyl
         Varied concentration in Hexane -       (9 components)
         M-EPA680PCB1J99-1ML              1mL Ampule

         PCB CONGENER MIXTURE #2
         EPA METHOD 680
         100ug/mL     3,3’,4,4’-Tetrachlorobiphenyl
         200ug/mL     2,2’,3,3’,4,5,5’,6,6’-Nonachlorobiphenyl
         100ug/mL     2,2’,4,6,6’-Pentachlorobiphenyl
         Varied concentration in Hexane -      (3 components)
         M-EPA680PCB2J99-1ML              1mL Ampule



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