Page 177 - Chem Service 2016 Catalogue
P. 177

METHOD 1660 - PYRETHRINS & PYRETHROIDS
          Method 1660 is applicable to the determination of pyrethrins and pyrethroids in municipal and industrial wastewater by extraction and
          high-performance liquid chromatography (HPLC) with an ultra-violet detector (UV).  Separation and measurement of the pyrethrins and pyrethroids
          is performed by reverse-phase Cl8 column HPLC with a multiple-wavelength UV detector.
     EPA1600  EPA METHOD 1660                                  EPA METHOD 1660                  Permethrin
                                                               PYRETHRINS & PYRETHROIDS MIXTURE #2
         PYRETHRINS & PYRETHROIDS MIXTURE #1
                                                                             Resmethrin
                                                               Allethrin
         400ug/mL
                        Cyfluthrin
                        d-(cis-trans)-Phenothrin
         400ug/mL
                                                               400ug/L in Acetonitrile      (3 components)
         200ug/mL
                        Fenvalerate
         400ug/mL
                        Tetramethrin
                                                               PYRETHRUM STANDARDS
         Varied concentration in Acetonitrile    (4 components)  M-PP16602A15-1ML    1mL Ampule
         M-PP16601A99-1ML                 1mL Ampule
                                                               EPA METHOD 1660
                                                               N-13151-100MG  Pyrethrum
                                                               S-13151A!-1ML     100ug/mL in Acetonitrile
                                                               S-13151T1-1ML    100ug/mL in tert-Butylmethylether
            METHOD 1663 - PETROLEUM HYDROCARBONS
          Method 1663 is applicable to the determination of petroleum hydrocarbons in municipal and industrial waster water by GC.  It may
          be used as a stand-alone method to determine the presence of diesel or crude oil.
         INTERNAL STANDARDS
         EPA METHOD 1663
         N-10203-1G        1,3,5-Trichlorobenzene
         S-10203J1-1ML     100ug/mL in Hexane
         S-10203J1-1ML     100ug/mL in Hexane
         S-10203X8-1ML     10000ug/mL in Methylene chloride
         S-10203X8-1ML     10000ug/mL in Methylene chloride
            METHOD 1664 - n-HEXANE EXTRACTABLE MATERIAL
          Method 1664 is applicable to the determination of n-Hexane extractable material (HEM) that is not adsorbed by silica gel (SGT-HEM) in
          municipal and industrial wastewaters.  Extractable materials that may be determined  are non-volatile hydrocarbons, vegetable oils, animal fats,
          waxes, soaps, greases, and related materials, as well as materials other than aliphatic petroleum hydrocarbons.  This method was developed
          to replace previously used gravimetric procedures that employed Freon 113, (a Class I CFC), as the extraction solvent for the determination
          of oil, grease and petroleum hydrocarbons by extraction and gravimetry.

         OIL & GREASE SPIKING MIXTURE
         EPA METHOD 1664, TPH
         n-Hexadecane
         Stearic acid
         4000ug/mL in Acetone             (2 components)
         M-OG16641B12-1ML                 1mL Ampule
            METHOD 1666 - VOLATILE ORGANIC POLLUTANTS

          Method 1666 is applicable to the determination of volatile organic pollutants specific to the Pharmaceutical Manufacturing Industry (PMI) that
          are amenable to purge-and-trap gas chromatography/mass spectrometry (GC/MS) or direct aqueous injection (GC/MS).
         STOCK STANDARD MIXTURE #1
         EPA METHOD 1666
         1000ug/mL      4-Methyl-2-pentanone         1000ug/mL         Isopropyl alcohol
         2500ug/mL      n-Butyl alcohol              2500ug/mL         n-Amyl alcohol
         2500ug/mL      tert-Butyl alcohol           2500ug/mL         Isobutyraldehyde
         2500ug/mL      Furfural
         Varied concentration in Water    (7 components)
         M-EPA1666SS1F99-1ML              1mL Ampule
         STOCK STANDARD MIXTURE #2
         EPA METHOD 1666
         1000ug/mL      p-Xylene                     2500ug/mL         Methyl formate
         1000ug/mL      m-Xylene                     1000ug/mL         Tetrahydrofuran
         1000ug/mL      n-Hexane                     1000ug/mL         Cyclohexane
         1000ug/mL      n-Heptane                    1000ug/mL         Trifluoromethane
         1000ug/mL      o-Xylene
         Varied concentration in Methanol    (9 components)
         M-EPA1666SS2M99-1ML              1mL Ampule




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