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Suguna Management System      Ver 1.0 / SOP / FQL / P3 - 09  Page  1 of 1



























           9. Determination of Castor oil in Oils in other Oils


                                                                   petroleum ether (boiling rang.40º C to 60º C or 60º
           SCOPE
                                                                   C to 80 º C).
           Applicable to test of all type of Oil.
                                                                FSulphuric  acid  molybdate  -  In  100  ml  of
                                                                   concentrated sulphuric acid dissolve 1.25 gm of
           OBJECTIVE
           This procedure is for the determination of Castor oil in   ammonium molybdate.
           Vegetable oils.
                                                                PROCEDURE
                                                                FTake 1.0 ml of the oil in clean and dry test tube.
           APPARATUS
           FTest tube
                                                                FAdd  10  ml  of  Acidified  Petroleum  ether.  Shake
           FHot plate                                              vigorously for 2 minutes and add one drop (0.5ml)
                                                                   of the ammonium molybdate reagent.
           FBeaker 250 ml
                                                                FThe  presence  of  castor  oil  indicates  by  white
           FRefuse unit.                                           turbidity in the solution.


           REAGENTS
                                                                REFERENCE:
           FAcidified  petroleum  ether:  Add  2  ml  of        IS 548-1976.
              concentrated  hydrochloric  acid  to  100  ml  of

























          Prepared by :                                                             Approved by :
                                                            131                                    Director - Technical
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