Page 11 - Parker - High purity chemicals in electronic application
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Absorber
                                                                                                                                     Column
                                                                                                                                                  Acid
                                                                                                                                                       DI Water
                                                               Storage
                                                                Tank
                                             Distillation
                                        Distillation
                                                                                                                                 Purier
                                                                                                                                 Column
                           Hydrolyzer
                                                                                                                        Sulfur Trioxide
                                                                                                                          Vaporizer
                                            Isopropyl Alcohol
                                                                                                                    Liquid
                                                                                                                  Sulfur Trioxide
                                                                                                                                                                                         Degasication
                                                                                                                                                                             Storage Tank
                                                                                                                    Storage
               Absorber
                                                                                                          Condensor
                                                                                                                                                                                                            UV
                     Sulfate
                     Esters
                                                                                                  Sulfur Trioxide
                                                                                                   Evaporator
                                                                                                                                                                 Reverse
                                                                                                                                                                 Osmosis
                                                                                                                                                                 System 2
                                  DI Water
                                                                                                                                                     Osmosis
 Propene
                                                                                                                                                     System 1
                                                                                                                                          Tank
                                                                                                                                                                                                      Ion
             Sulfuric
                                                                     Ultapure
                                                                                                                                                        Ultra-Pure Water
              Acid
                                                                     Dilute HF
                                                                                                                                                                                        Storage
                                                                                                                                                                                         Tank
                                                                                                                                                                                         & Air
        High-Purity Acids & Bases                                                                 Oxidizer  Sulfur Trioxide  Water UHP Sulfuric Acid  Pretreatment  Dilution Reverse  Introduction Exchange & Air Vent Filter  Vent Filter  Exchange  Station EDI
                       DI Water
                                                                                                                                                                         Ion
                                                                                                                         3
                                                                                           O2
                                                                                         Rich Air                Recycle
        Hydrogen Peroxide                                                                                   2
                                                   Storage
                                                   Ultrapure      DI Water     Hydrogenator                                                                   Schematic
                                                  Aquesous HF                                                                           4
 Anhydrous HF                              Final
                                                                                                             Solvent
                                   Hydrouoric Acid
        Hydrogen peroxide is made in a series of steps.               Hydrogen           2                  Purication
                                         Distillation
        A hydrocarbon-based “work-solution” is fed to
                            Concentrated
        the hydrogenator along with a stream of hydrogen                                                                                                      Selection Process
                            Aqueous HF
        where hydrogenation occurs over a bed of Ni                                                                         Liquid
        or Pd catalysts.                                                    1   Hydrogen Peroxide                           Extractor
        The first filtration step is used to capture catalyst   Anthraquinone
                                                        + Solvent
        particles from the hydrogenated fluid.                                                                2                                               Applications
                                                                                            Column 2
                                                                                                      Column 1
        In the oxidizer, oxygen-rich air is introduced to the       2                      Purication  Purication                                           Ultra-Pure
        work solution to reverse the previous reaction.                                                                                                       Water (UPW)
        The resulting work-solution contains about 40%
        H 2 O 2  by weight as it goes into the liquid extractor.
        Water is fed into the extractor and since the H 2 O 2                                                                                                 High-Purity
        is miscible in water while the solvent is not, the                                                                                                    Solvents Isopropyl
                                                                                                                                                              Alcohol (IPA)
        water-peroxide layer can be removed and sent to
        the purification columns.                     Core Filter(s)  Location    Purpose         Features              Benefits          Advantages          High-Purity
        In the purification columns, the water-peroxide   Abso-Mate                                                                                           Acids & Bases
        mixture is further concentrated and purified. For   Poly-Mate                                                                                         Hydrouoric Acid
        UHP hydrogen peroxide, multiple columns may                             Incoming raw   Polypropylene depth   Capture large particles    Protection of
        be used.                                     Poly-Mate Plus      1       materials         media             in raw materials      evaporator         High-Purity
                                                        Polyflow                                                                                              Acids & Bases
                                                       Polyflow-G                                                                                             Sulfuric Acid
                                                      Chemflow-PE                                                                                             High-Purity
                                                   Chemflow-PE Select              Stage/     PTFE membrane on                           Process particle     Acids & Bases
                                                                         2      pre-filtration/  either HDPE or PP   Fine particle removal                    Hydrogen Peroxide
                                                       Proflow II-E               blending     support structure                            control
                                                    Proflow II-E Select
                                                      Clariflow-WE                                                                      Provide consistent    Services
                                                                                                                  Removal of particles in
                                                       Clariflow-E       3        DI water      Hydrophilic PES   UPW down to 0.02 microns  source of UPW to
                                                                                                  membrane
                                                    Clariflow-E Select                                                                    liquid reactor
                                                      Chemflow-PE
                                                   Chemflow-PE Select                         PTFE membrane on                          Final filtration step   Selection Matrix
                                                                                   Final
                                                       Proflow II-E      4                    either HDPE, PP or   Fine particle removal  to help meet product
                                                                                  Package
                                                    Proflow II-E Select                      PFA support structure                        specifications
                                                       Fluoroflow                                                                                             Product Overview
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