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Suguna Management System      Ver 1.0 / SOP / FQL / P2 - 36  Page  1 of 1



























           36. Estimation of Potassium Chloride Assay



           SCOPE                                                PROCEDURE
           To estimate the assay of Potassium chloride.         1. Take 0.2gm of Potassium chloride sample in 250ml
                                                                   of conical flask.
           APPARATUS
                                                                2. Add100 ml of distilled water + 3ml of Potassium
           FAnalytical Balance, 1 mg  / 0.1 mg accuracy
                                                                   Chromate.
           FConical flask, 250 ml
                                                                3. Titrate  with  0.1N  silver  nitrate  until  solution
           FBurette, 10 ml                                         becomes brown colour.
           FGraduated pipette, 10 ml, 5 ml                      4. Run the blank without taking sample.

                                                                Note:  Each  1  ml  of  0.1N  AgNo3  is  equivalent  to
           REAGENTS
                                                                74.55mg of potassium chloride.
           F0.1N Silver nitrate: Dissolve approximate 1.699g
              of  silver  nitrate,  AR  grade  in  distilled  water  and
              made up to 100 ml
           F5% Potassium chromate.




           CACULATION

                                                          TV-B x N.of AgNO3 X 74.55 X 100
                                 Assay = ---------------------------------------------------------------
                                                                      Sample weight, g















          Prepared by :                                                             Approved by :
                                                            113                                    Director - Technical
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